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The photoreaction generating the sequence-defined macromolecules is based on a monomer library (Fig. 1a), in which each monomer carries a photoreactive benzaldehyde function as well as an ene functionality required for the photochemically induced Diels–Alder reaction. Contrary to our previous report—which employed two monomer types with separate diene and dienophile functions53—the herein presented monomers entail a dual diene/dienophile character.
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