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A set of speciation experiments was conducted with a CH COONa solution at 300?°C and 2.4–3.5?GPa using a membrane-type diamond anvil cell37, mounted with ultra-low fluorescence anvils with a 500??m-diameter culet. The starting fluid was prepared by mixing 5.00?ml of 1.0?mol?l?1 NaOH (Merck KGaA) and 0.286?ml of pure CH COOH (Merck KGaA, 100% purity, density=1.05?kg?l?1) solutions.
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