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Three new metal chalcogenides have been identified in Mn (Gd In )S with N = 3, 4, and 5 via a flux-growth synthesis. All compounds crystallize in the same space group of orthorhombic Cmcm with cell constants: Mn GdInS (1), a = 3.789(1) Å, b = 12.411(1) Å, and c = 15.489(1) Å; Mn Gd S (2), a = 3.778(1) Å, b = 12.505(2) Å, and c = 19.114(2) Å; Mn Gd S (3), a = 3.769(1) Å, b = 12.466(2) Å, and c = 22.289(3) Å.
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