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Abstract This study presents the synthesis and characterization of three novel metal chelates: Ni(DTHMN) (1), Co(DTHMN) (2), and Fe(DTHMN) (3). Comprehensive analytical techniques, including elemental analysis, infrared (IR) and electronic (UV-Vis) spectroscopy, thermal analysis, molar conductivity, and magnetic susceptibility measurements, were employed to investigate their structural and electronic properties.
Abstract Hydrazones and their metal complexes have acquired a lot of interest because of their various biological and catalytic applications. The reaction of the symmetrical hydrazone (NBHD) with Cu(II) salts, including Cl−, Br−, and SO42−, has been investigated. The structures of Cu-NBHD complexes were explored by using various spectroscopic and analytical tools.
Supporting Information Filename Description aoc7752-sup-0001-Supplementary_Data.docxWord 2007 document , 66.9 KB Table S1 Thermal gravimetric results of the metal complexes. Table S2. Solvent parameters analyzed by linear solvation energy relationships (LSFER). Figure S1. The relation between νStoke/cm−1 vs FL-M. Figure S2. The relation between νStoke/cm−1 vs FB. Figure S3. The relation between νStoke/cm−1 vs FK-C-V. Figure S4. The relation between νStoke/cm−1 vs ETN. Table S3.
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