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The development of efficient heterogeneous Fenton catalysts is mainly by “trial-and-error” concept and the factor determining H O activation remains elusive. In this work, we demonstrate that suitable facet exposure to elongate O–O bond in H O is the key parameter determining the Fenton catalyst’s activity. CuFeO nanocubes and nanoplates with different surface facets of {110} and {012} are used to compare the effect of exposed facets on Fenton activity.
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