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2. Materials and Methods 2.1. Reagents and Standard Solutions The standards of AFB1, AFB2, T-2, HT-2, OTA, ZEN, and α-ZEL were obtained from Sigma (West Chester, PA, USA) and Fluka (West Chester, PA, USA), all with purity higher than 97%. DON, DON-3-G, DOM-1, and FB1 were also purchased from Sigma, with purity higher than 92.5%. The surrogate standard ochratoxin A-(phenyl-d5) (OTAd5) was purchased from Sigma at 10 mg/L, with purity higher than 95%.
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