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Articles by Jared A. Pienkos
Oxidatively Stable Ferrocenyl-π-bridge-Titanocene D-π-A Complexes: An Electrochemical and Spectroscopic Investigation of the Mixed-Valence States
The synthesis, spectroscopic, and electrochemical characterization of oxidatively stable D-π-A compounds of the form (Me2CpC2Fc)2TiCl2 and RCp2Ti(C2Fc)¬2CuX (where Fc = ferrocenyl) are reported. Oxidative stability enabled by the addition of CuX is evidenced by voltammagrams of the RCp2Ti(C2Fc)2CuX compounds which all display two chemically-reversible 1e- FeIII/II couples, indicative of electronic communication between the Fc- termini.
Enantioenriched Molybdenum Dearomatization: Dissociative Substitution with Configurational Stability
The preparation and properties of the complex (R ,R)-MoTp(NO)(DMAP)(?2-?-pinene) are described (?10 g scale; DMAP = 4-(dimethylamino)pyridine; Tp = hydridotris(pyrazolyl)borate). This complex undergoes exchange of the pinene with a wide range of other ? ligands including acetone, ethyl acetate, N,N-dimethylformamide, acetonitrile, and naphthalene.
A trans-bidentate bis-pyridinyl ligand with a transition metal hinge
N. C. Vieira, J. A. Pienkos, C. McMillen, A. R. Myers, A. P. Clay and P. S. Wagenknecht, Dalton Trans., 2017, Accepted Manuscript , DOI: 10.1039/C7DT03252H If you are not the author of this article and you wish to reproduce material from it in a third party non-RSC publication you must formally request permission using RightsLink. Go to our Instructions for using RightsLink page for details.
Synthesis of Novel Hexahydroindoles from the Dearomatization of Indoline
In a preliminary communication, it was reported that TpW(NO)(PMe)(η-benzene) () could be combined with analkylindoline and an ammonium triflate salt to form an η-indolinium complex ( Scheme ). (23) This system has the ability to react with electrophiles to give a stable, double cationic species (), which can then react with nucleophiles to form a tetrahydroindolium complex ().
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