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Abstract X-ray dynamic tomographic microscopy offers new opportunities in the volumetric investigation of dynamic processes. Due to data complexity and their sheer amount, extraction of comprehensive quantitative information remains challenging due to the intensive manual interaction required.
Understanding electrical percolation and charging mechanisms in electrochemically active biphasic flowable electrodes is critical for enabling scalable deionization (desalination) and energy storage. Flowable electrodes are dynamic material systems which store charge (remove ions) and have the ability to flow. This flow process can induce structural changes in the underlying material arrangement and result in transient and non-uniform material properties.
Figure 1a schematically depicts the measurement setup. We construct an electrochemical cell for operando XTM, consisting of a polyether ether ketone cell housing tube and two steel current collectors. The system we investigate here consists of two, 250 μm-thick electrodes of platelet-shaped graphite particles spaced with a 250 μm-thick glass fibre separator.
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