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Direct N-methyl C−H esterification of O-tosyl hydroxamates to enable facile synthesis of hemiaminal esters† Here we present a new method for synthesizing amide hemiaminal esters through the direct N-methyl C−H esterification of O-tosyl hydroxamates. This approach demonstrates good tolerance for a variety of functional groups and operates under mild, transition-metal-free conditions, thus providing an accessible and effective pathway to hemiaminal esters.
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