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Electrochemical Minisci reaction via HAT-driven α-C(sp3)−H functionalization of alcohols Heng Li, Jinwen Tong, Yan Zhu, Cong Jiang, Ping Liu and Peipei Sun Abstract An efficient electrochemical Minisci reaction to access 3-hydroxyalkylquinoxalin-2(1H)-ones involved hydrogen atom transfer (HAT) driven α-C(sp3)−H functionalization of alcohols was achieved.
Visible-light-induced dehydrogenative sulfonylation of tertiary amines under transition-metal- and photocatalyst-free conditions An efficient dehydrogenative sulfonylation of tertiary amines with thiosulfonates enabled by visible-light irradiation is developed. This protocol allows for the construction of a variety of cyclic and acyclic β-sulfonyl enamines under transition-metal-free, external oxidant-free, photocatalyst-free and mild reaction conditions.
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