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Simple tin derivatives, Cp* SnCl (1) and Ph SnCl (2), catalyze the hydrophosphination of alkene substrates with diphenylphosphine. Competitive dehydrocoupling to give Ph P was observed, but this side reaction can be mitigated when the catalysis is conducted under an H atmosphere. Efforts to prepare stable tin bis(phosphido) compounds commonly resulted in decomposition to Ph P . Lewis acidic inorganic tin compounds do not show dehydrocoupling reactivity.
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