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Articles by Lukas Link
Filling Voids: Cubic Carbodiimide Nitride Nitridometalates (Ba6Nx)2[MN4][CN2]6 of M = Zr, Hf, Nb, Ta, Mo, and W
1 Introduction Compounds containing the carbodiimide anion [NCN]2− increasingly entered the focus of research interest during the last decades, for example, due to their promising luminescence properties or their potential application in lithium or sodium ion batteries.[1] For these purposes, mostly pseudo-binary or pseudo-ternary compounds containing at least one transition metal cation were scrutinized.
Nitridogermanates(IV): The Germanide Oxide Sr15Ge[GeN4]3O, the Carbodiimide Ba5[GeN4][CN2] and the Oxidonitridogermanate Sr6[Ge2N6O]
We have encountered various novel compounds by serendipity, due to small oxygen or carbon impurities, during our explorative studies to explore the crystal chemistry of multinary germanium nitrides and nitridogermanates.
Reactions of Binary Nitrides in Liquid Hydrogen Fluoride and the First Calcium Oxidofluoridometallate of a Group Six Element Ca[Mo2O2F9]2 ⋅ HF
Introduction Oxidofluoridometallates of Mo and W can be synthesized by the controlled hydrolysis of the respective metal hexafluoride.1, 2 This is usually achieved by the reaction between SiO2 and anhydrous HF (aHF) as it is known to liberate defined amounts of H2O slowly:1-3 (1) (2) We wanted to explore if a controlled ammonolysis was also possible in aHF in analogy to this controlled hydrolysis.
Frontispiece: The Reduced Nitridogermanates(III) Ca6[Ge2N6] and Sr6[Ge2N6] with Ge−Ge Bonds
Frontispiece Dr. Peter Höhn Corresponding Author peter.hoehn@cpfs.mpg.de Chemical Metals Science, Max Planck Institute for Chemical Physics of Solids, Nöthnitzer Str. 40, 01187 Dresden, Germany Search for more papers by this author PDF ShareShare Abstract Nitridogermanates In their Research Article on page 7691, Peter Höhn, Rainer Niewa et al.
The Reduced Nitridogermanates(III) Ca6[Ge2N6] and Sr6[Ge2N6] with Ge−Ge Bonds
Abstract The first nitridogermanates(III) Ca6[Ge2N6] and Sr6[Ge2N6] were synthesized from sodium flux and structurally characterized by powder and single crystal X‐ray diffraction, respectively. They crystallize isostructurally to each other and homeotypic to Ca6[Cr2N6]H in space group R . They feature unprecedented, mutually isolated, ethane‐like [GeIII2N6]12− anions in a staggered conformation.
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