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Ammine metal borohydrides (AMBs) have recently commanded attention as low-temperature hydrogen sources. As an alternative to widely used mechanochemical synthesis that affords mixtures with salt co-products, we have been investigating solution synthesis routes to obtain pure AMBs. Here we show that reactions of MCl + nNaBH with ammonia in thf afford ammonia-borane (AB) via borane abstraction from M-coordinated borohydride.
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