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Hexacoordinate Germanate Metal-Organic Frameworks for the Detection of Pb2+ ions in Aqueous Solution Hexacoordinate silicate and germanate linkers supporting high negative charges have been prepared and applied as building blocks for anionic MOF frameworks with lanthanide metal-based nodes.
The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.orglett.7b03841.General experimental; Optimization of TMOS loading; Experimental details and characterizing data for compounds; Copies of 1H and 13C spectra for all compounds; HPLC analysis for amide 26; In situ observation of the de facto acylating agent by 1H, 13C, and 29Si NMR; Green metrics (PDF)
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