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The buried solid/liquid interface between hydrophilic fused silica and binary solvent mixtures of acetonitrile (MeCN) and methanol (MeOH) was studied with vibrational sum-frequency generation (vSFG) spectroscopy. Our data showed that at high relative concentrations of methanol, the Fermi resonance peak in the vSFG spectrum is greatly suppressed, and it progressively gains intensity as methanol is diluted with perdeuterated acetonitrile.
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