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The multi-shelled MgCo O hollow microspheres (MCO) with the spinel structure as an anode material for lithium ion batteries are prepared through a solvothermal process using colloidal carbon spheres as a template, followed by calcination process in air. The multi-shelled MgCo O hollow microspheres are synthesized via the heterogeneous contraction by non-equilibrium heat balance owning to temperature gradient.
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