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Articles

Fluorine-18 labelled Ruppert-Prakash reagent ([18F]Me3SiCF3) for the synthesis of 18F-trifluoromethylated compounds

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By Anna Pees, Amsterdam UMC, BV Cyclotron VU, Maria J.W.D Vosjan
| Royal Society of Chemistry Verified
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Correction: Fast and reliable generation of [18F]triflyl fluoride, a gaseous [18F]fluoride source

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By A. Pees, C. Sewing, BV Cyclotron VU, V. Tadino
| Royal Society of Chemistry Verified
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Fast and reliable generation of [18F]triflyl fluoride, a gaseous [18F]fluoride source

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By A. Pees, C. Sewing, BV Cyclotron VU, V. Tadino
| Royal Society of Chemistry Verified
A novel strategy for the production of reactive [ F]fluoride has been developed, omitting time consuming azeotropic drying procedures. Gaseous [ F]triflyl fluoride is formed instantaneously at room temperature from hydrated [ F]fluoride, followed by distillation in less than 5 minutes into a dry aprotic solvent, in which dry [ F]fluoride is released in presence of base with >90% radiochemical yield.
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