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Dajana Barisic on Muck Rack

Dajana Barisic

As seen in: Royal Society of Chemistry
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Deuteration of Pd-activated C(sp2)-H bonds in the Solid State

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By Dajana Barisic, Ivan Halasz, Stipe Lukin, Alen Bjelopetrović
| Royal Society of Chemistry Verified
Deuteration of Pd-activated C(sp2)–H bonds in the Solid State We report mechanochemically-induced deuteration of Pd-activated aromatic C(sp2)–H bonds at ambient temperature under solvent-free conditions. Deuterium was sourced from cysteine-d4 to obtain mono- or dideuterated products from various aromatic palladacycles. Next to good deuteration yields, based on time-resolved in-situ Raman monitoring and DFT calculations, we present a detailed view of the reaction course in the solid state.
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