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Elya Kandahari on Muck Rack

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Electrochemical Activation of α-Carbonyl Alkoxyamines for Direct Nucleophilic Substitution

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By John Putziger, Song Lin, Elya Kandahari
| dx.doi.org
2,2,6,6-Tetramethylpiperidin-1-oxyl (TEMPO)-derived alkoxyamines (alkyl-TEMPO) are frequently encountered in the methodology literature, most often obtained when the persistent aminoxyl radical TEMPO captures an in situ generated C-centered radical. (1,2) The utility of alkyl-TEMPO species has traditionally been limited to either oxidation to ketones using m-chloroperoxybenzoic acid or reduction to free alcohols using zinc.
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