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F. Kilgenstein

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Synthesis of heteroatomic bridged paracyclophanes

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By Fachbereich Chemie, K. Reuter, A. Reuter, F. Kilgenstein
| Royal Society of Chemistry Verified
Heteroatomic bridged paracyclophanes were obtained by two independent synthetic approaches. The required precursors consist of para R SiCl (R = Me, iPr) substituted aromatic rings (2 and 4). They were subsequently functionalised by using NH , [LiPH (dme)] or LiAl(PH ) . In the case of the Me-substituted species 2, the reaction with NH directly yielded the Si N bridged paracyclophane 5.
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