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Visible‐Light‐Induced Mpg‐C3N4 Catalyzed C(sp2)−H Thiocyanation of Ketene Dithioacetals
Using mesoporous graphite carbon nitride (mpg-C N ) as metal-free heterogeneous catalyst, the thiocyanation of ketene dithioacetals was achieved under visible light irradiation with oxygen as green oxidant and without any other additives. The present protocol has excellent functional group tolerance and the desired tetrasubstituted alkenyl thiocyanides were obtained in moderate to good yields.
Visible‐Light‐Induced Mpg‐C3N4 Catalyzed C(sp2)‐H Thiocyanation of Ketene Dithioacetals
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