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Articles

De Novo Synthesis and Structural Elucidation of CDR-H3 Loop Mimics

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By Guangkuan Zhao, Alexis D. Richaud, R. Thomas Williamson, Michael Feig
| dx.doi.org
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Synthesis of 2-Substituted Indoles through Cyclization and Demethylation of 2-Alkynyldimethylanilines by Ethanol

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By Guangkuan Zhao, Vincent Gandon, Christelle Roudaut, Mouad ALAMI
| Royal Society of Chemistry Verified
Synthesis of 2-Substituted Indoles through Cyclization and Demethylation of 2-Alkynyldimethylanilines by Ethanol Herein, we demonstrated for the first time that 2-alkynyldimethylamines easily cyclize in EtOH according to a 5-endo-dig annulation into 2-substituted indoles without the aid of any additive or any metal catalyst to activate the triple bond.
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Unexpected Oxidative Ring Opening of Electron-Rich 3-Aminobenzofurans into α-Ketoimines Derivatives

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By Ilhem Khelifi, Guangkuan Zhao, Nour-Eddine Ghermani, Olivier Provot
| American Chemical Society
An unexpected ring opening of 3-aminobenzofurans promoted by NaOtBu in hot toluene, leading to a variety of α-ketoimines, is described. In the presence of 3-iodobenzofurans, NaOtBu mediates the 3-aminobenzofurans ring opening via a possible radical pathway without the help of any external radical sources.
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