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Istemi Kuzu on Muck Rack

Istemi Kuzu

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Articles

Hexaphenyl carbodiphosphorane adducts of heavier group 15 element trichlorides: syntheses, properties and reactivities

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By Istemi Kuzu, Nis-Julian H. Kneusels, Bastian Weinert
| Royal Society of Chemistry Verified
Hexaphenyl carbodiphosphorane adducts of heavier group 15 element trichlorides: syntheses, properties and reactivities Herein, we present the series of hexaphenyl carbodiphosphorane (CDPPh) adducts of heavier group 15 trichlorides ECl3 (E = P-Bi). The reaction with PCl3 yields the known salt [CDPPh−PCl2][Cl] ([1][Cl]), the heavier element trichlorides ECl3 (E = Sb (4), Bi (5)) give the neutral adducts CDPPh−ECl3 which were characterised crystallographically and spectroscopically.
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A New Anthraquinoid Ligand for the Iron-catalyzed Hydrosilylation of Carbonyl Compounds at Room Temperature: New Insights and Kinetics

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By Robert LANGER, Alvaro Raya-Baron, Carmen Piedad Galdeano-Ruano, Istemi Kuzu
| Royal Society of Chemistry Verified
The reaction of 1-((2-(pyridin-2-yl)ethyl)amino)anthraquinone with either Fe(HMDS)2 or Li(HMDS)/FeCl2 allowed the preparation of a new anthraquinoid-based iron(II) complex active in hydrosilylations of carbonyls. The new complex Fe(2)2 was characterized by single-crystal X-ray diffraction, infrared spectroscopy, NMR and high resolution mass spectrometry (electrospray ionization).
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