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Abstract In this research, a new series of thiazole-based hydrazone derivatives (9–14) was designed, synthesized, and evaluated for α-amylase inhibitory activity as a strategy to manage postprandial hyperglycemia in type 2 diabetes (T2DM). The target compounds were obtained via a two-step procedure: condensation of thiosemicarbazide with substituted aromatic aldehydes to form hydrazones, followed by cyclization with phenacyl bromide.
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