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Lourdes Ibarlucea on Muck Rack

Lourdes Ibarlucea

As seen in: Chemistry World
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Articles

(Diphenylphosphine)alkylaldehyde to afford hydride- or alkyl-[(diphenylphosphine)alkylacyl]rhodium(III) or (diphenylphosphine)alkylester complexes. Theoretical and experimental diastereoselectivity.

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By Susan Azpeitia, Claudio Mendicute-Fierro, Eider San sebastian, Lourdes Ibarlucea
| Royal Society of Chemistry Verified
(Diphenylphosphine)alkylaldehyde to afford hydride- or alkyl-[(diphenylphosphine)alkylacyl]rhodium(III) or (diphenylphosphine)alkylester complexes. Theoretical and experimental diastereoselectivity. MARIA ANGELES Angeles GARRALDA HUALDE, Susan Azpeitia, Montserrat Barquín, Claudio Mendicute-Fierro, Miguel A. A.
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A Pentacoordinated Norbornenyl-Acyl-Rhodium(III) Complex as a Likely Intermediate in the Catalytic Hydroacylation of Norbornadiene

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By José Seco, Naroa Almenara, Lourdes Ibarlucea, Claudio Mendicute-Fierro
| Chemistry World Verified
[RhCl(NCO)(nbyl)(PR3)] (nbyl = ?-norbornenyl; NCO = quinoline-8-acyl; R = p-F-C6H4) (1) has been synthesized by the reaction of [Rh(nbd)Cl]2 (nbd = norbornadiene) with 2 equivalents of NCHO (quinoline-8-carbaldehyde) and 2 equivalents of PR3. Compound 1 has been fully characterized in solution and also in the solid state by X-ray difraction. Compound 1 shows low stability in solution and undergoes slow ring closure isomerization to [RhCl(NCO)(ntyl)(PR3)] (ntyl = ?-nortricyclyl) (2) after 12 hours.
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