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Nmr CoRe NMR

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Reversible Parahydrogen Induced Hyperpolarization of 15N in Unmodified Amino Acids Unraveled at High Magnetic Field

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By Ewoud Vaneeckhaute, Nmr CoRe NMR, Univ Lyon CNRS, Jean-Max Tyburn
| Wiley Online Library Verified
2.4.3 Motifs V–IV Motif V (yellow) is highly similar to motif IV (light blue) but shifted from the chemical shift region with an N-bonded axial ligand to the region associated with O-bonded axial ligands. Motif V is thus assigned to a complex with ammonia and N-bonded alanine occupying the equatorial ligand positions and O-bonded alanine occupying the axial position (Figure 4d,V). In motif VI (red), the patterns revealing ammonia and N-bonded alanine are mirrored as compared to motif V.
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