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Ethylene Copolymerization with 4-Methylcyclohexene or 1-Methylcyclopentene by Half-Titanocene Catalysts: Effect of Ligands and Microstructural Analysis of the Copolymers - Macromolecules (ACS Publications)

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By Antonella Caterina Boccia, Hitoshi Harakawa, Srisuda Patamma, Laura Boggioni
| American Chemical Society
Ethylene copolymerizations with 4-methylcyclohexene (4-MeCHE) or 1-methylcyclopentene (1-MeCPE) have been explored by the aryloxo- or ketimide-modified half-titanocenes, Cp?TiCl (X) [X: O-2,6-iPr C H ; Cp?: 1,2,4-Me C H (1), tBuC H (2), C Me (Cp*); X: N?CtBu ; Cp?: tBuC H , Cp, indenyl], linked half-titanocenes, [Me Si(C Me )(NR)]TiCl (R = tBu, cyclohexyl), and ordinary metallocenes, [Et(indenyl) ]ZrCl , Cp ZrCl , in the presence of methylaluminoxane (MAO) cocatalyst.
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