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Xavier Just‐Baringo on Muck Rack

Xavier Just‐Baringo

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Biocatalytic Conversion of Cyclic Ketones Bearing α‐Quaternary Stereocenters into Lactones in an Enantioselective Radical Approach to Medium‐Sized Carbocycles - Morrill - - Angewandte Chemie International Edition - Wiley Online Library

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By Gideon Grogan, Charlotte Morrill, Chantel Jensen, Xavier Just‐Baringo
| Arthritis & Rheumatology Verified
Cyclic ketones bearing α‐quaternary stereocenters underwent efficient kinetic resolution using cyclohexanone monooxygenase (CHMO) from Acinetobacter calcoaceticus. Lactones possessing tetrasubstituted stereocenters were obtained with high enantioselectivity (up to >99 % ee) and complete chemoselectivity. Preparative‐scale biotransformations were exploited in conjunction with a SmI2‐mediated cyclization process to access complex, enantiomerically enriched cycloheptan‐ and cycloctan‐1,4‐diols.
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