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Articles

Formal Diels–Alder reaction of saturated carboxylic acids via C–H activation - Nature Chemistry

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By Qiyuan He, yilin lu, Tao Sheng, Nikita Chekshin, Jie-Lun Yan, Tao Zhang, Jin-Quan Yu
| Nature Verified
Abstract Constructing ubiquitous bridged bicyclic scaffolds from simple aliphatic feedstocks via multiple C(sp3)–H functionalizations is a significant challenge in organic synthesis, demanding powerful catalysts capable of precise selectivity control. Here we demonstrate a catalytic system that enables abundant cyclic carboxylic acids to couple with dienophiles in a formal Diels–Alder manner with exclusive regioselectivity, forging bridged bicyclic scaffolds.
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Synthesis of Spiro Carbocycles via Methyl β-C(sp3)–H Functionalization of Cyclic Aliphatic Acids

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By Tao Sheng, Zhihan Zhao, yilin lu
| dx.doi.org
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Synthesis of Spiro Carbocycles via Methyl β-C(sp3)–H Functionalization of Cyclic Aliphatic Acids

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By Tao Sheng, Zhihan Zhao, yilin lu
| ACS Publications
Cite Jump to ExpandCollapse ArticleFebruary 14, 2026 Synthesis of Spiro Carbocycles via Methyl β-C(sp3)–H Functionalization of Cyclic Aliphatic Acids Click to copy article linkArticle link copied! Tao Sheng Tao Sheng Department of Chemistry, The Scripps Research Institute, 10550 N. Torrey Pines Road, La Jolla, California 92037, United States Zhihan Zhao Zhihan Zhao Department of Chemistry, The Scripps Research Institute, 10550 N.
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