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Manufacturing of Novel Nanostructured TiCrC Carbides Using Mechanical Alloying and Spark Plasma Sintering
3.1. Characterization of Bulk Samples Prepared via SPS XRD results of the milled powders and spark-plasma-sintered samples produced from different milling times are presented in Figure 1. As can be observed, the un-milled powder mixture’s XRD pattern, used as a reference, exhibits all of the expected Bragg peaks for the initial elements (Ti, Cr, and C). Nine Bragg peaks are visible in the Ti phase, and the remaining peaks belong to both the Cr and C phases.
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