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Submitted: 02 October 2026 You are already at the latest version A Quinazolinones are privileged N‑heterocycles with broad pharmaceutical relevance, yet catalyst‑free synthesis from readily available 1,3‑diketones remains challenging.
Inorganic ligand-supported Mo oxide as a hydrogen atom transfer photocatalyst for direct C(sp2)−H phosphorylation Visible-light-induced C(sp2)−H phosphorylation of 2H-thiozoles/quinoxalines with H-phosphine oxides was achieved by using an inorganic-ligand supported Mo oxide ([N(C4H9)4]2[Mo6O19]) as a hydrogen atom transfer (HAT) photocatalyst.
Aerobic Oxidative C-H Phosphorylation of Quinoxalines under Catalyst-free Conditions We herein report one direct and efficient protocol on phosphorylation of quinoxalines, which employs aerobic oxygen as the green oxidant under catalyst-free conditions. This methodology represents one of the most environmental-friendly and easily-handled protocols, providing a series of phosphorylated quinoxalines in good to excellent yields.
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